Science of Synthesis: Houben-Weyl Methods of Molecular Transformations, 第 35 卷Ernst Schaumann Thieme, 2000 - 850 頁 Science of Synthesis: Houben-Weyl Methods of Molecular Transformations is the entirely new edition of the acclaimed reference series Houben-Weyl, the standard synthetic chemistry resource since 1909. This new edition is published in English and will comprise 48 volumes published between the years 2000 and 2008. Science of Synthesis is a quality reference work developed by a highly esteemed editorial board to provide a comprehensive and critical selection of reliable organic and organometallic synthetic methods. This unique resource is designed to be the first point of reference when searching for a synthesis strategy.
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第 1 到 3 筆結果,共 79 筆
... washed with CH2Cl2 ( 3 × 100 mL ) . The combined organic layers were dried ( Na2SO4 ) and the solvent was removed . Flash chromatography ( silica gel ) of the residue gave the title compound ; yield : 247 mg ( 80 % ) . 3 - Chloro - 3 ...
... washed with H2O and dried ( MgSO4 ) . The pentane was removed under reduced pressure and the product was purified by distillation ; yield : 60-90 % . 1,2 - Dibromoalkanes ( 90 ) ; General Procedure : [ 278,288 ] To a soln of the alkene ...
... washed with aq Na2SO , soln , and dried ( MgSO4 ) . Remov- al of the solvent under reduced pressure left the crude product , which was purified by column chromatography ( silica gel ) ; yield : 50–99 % . 1 - Bromoalkan - 2 - ols 97 ...