Science of Synthesis: Houben-Weyl Methods of Molecular Transformations, 第 35 卷Ernst Schaumann Thieme, 2000 - 850 頁 Science of Synthesis: Houben-Weyl Methods of Molecular Transformations is the entirely new edition of the acclaimed reference series Houben-Weyl, the standard synthetic chemistry resource since 1909. This new edition is published in English and will comprise 48 volumes published between the years 2000 and 2008. Science of Synthesis is a quality reference work developed by a highly esteemed editorial board to provide a comprehensive and critical selection of reliable organic and organometallic synthetic methods. This unique resource is designed to be the first point of reference when searching for a synthesis strategy.
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... temperature range . The high relative C - H reactivity index has been attributed to the trichloromethylsulfanyl ... temperature of the distillation vessel must be kept below 125 ° C ; above this temperature , ( Cl , CS ) , decomposes ...
... temperature to -30 ° C . Further Cl2 was added at such a rate that the reaction temperature varied between -35 and -30 ° C , and the color of the mixture remained as little yellow as possible . After Cl2 addition was complete ( 5-6 h ) ...
... temperature 51 ° C ) ( CAU- TION ) . The bath temperature was then raised to 58-61 ° C over 30 min and portions of POCI , ( 3 × 25 mL ) were added at 45 - min intervals , followed by the addition of further POCI , ( 80 mL ) and a ...