Science of Synthesis: Houben-Weyl Methods of Molecular Transformations, 第 35 卷Ernst Schaumann Thieme, 2000 - 850 頁 Science of Synthesis: Houben-Weyl Methods of Molecular Transformations is the entirely new edition of the acclaimed reference series Houben-Weyl, the standard synthetic chemistry resource since 1909. This new edition is published in English and will comprise 48 volumes published between the years 2000 and 2008. Science of Synthesis is a quality reference work developed by a highly esteemed editorial board to provide a comprehensive and critical selection of reliable organic and organometallic synthetic methods. This unique resource is designed to be the first point of reference when searching for a synthesis strategy.
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第 1 到 3 筆結果,共 86 筆
... stirring was discontinued and the thick , colorless solid that formed was allowed to stand for 40 min . The alcohol ( 0.174 mol ) was then added and the mixture was stirred for 20 min , before being distilled . Fractions of boiling ...
... stirred suspension of NaNO2 ( 105 g , 1.5 mol ) in 3 - ethylpent - 2 - ene ( 115 mL , 84 g , 0.85 mol ) and MeOH ( 450 mL ) maintained at -15 to -5 ° C . After stirring for another 3 h , the mixture was poured into cold H2O ( 2 L ) ...
... stirred , refluxing , dried suspension of the Na salt of N - hydroxypyridine - 2 ( 1H ) -thione ( 1.8 g , 12 mmol ) and DMAP ( 120 mg , 1 mmol ) in BrCCl ( 100 mL ) . The reaction was monitored by TLC , and after completion the mixture ...