Science of Synthesis: Houben-Weyl Methods of Molecular Transformations, 第 35 卷Ernst Schaumann Thieme, 2000 - 850 頁 Science of Synthesis: Houben-Weyl Methods of Molecular Transformations is the entirely new edition of the acclaimed reference series Houben-Weyl, the standard synthetic chemistry resource since 1909. This new edition is published in English and will comprise 48 volumes published between the years 2000 and 2008. Science of Synthesis is a quality reference work developed by a highly esteemed editorial board to provide a comprehensive and critical selection of reliable organic and organometallic synthetic methods. This unique resource is designed to be the first point of reference when searching for a synthesis strategy.
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... mmol ) was added in portions with stirring to a soln of the alcohol 5 ( 10 mmol ) in CH2Cl2 ( 25 mL ) at 0 ° C . A soln of Et3N ( 2.79 mL , 20 mmol ) and DMAP ( 24 mg , 0.2 mmol ) in CH2Cl2 ( 5 mL ) was then added dropwise with stirring ...
... mmol ) , NBS ( 1.12 g , 6.3 mmol ) , and DBPO ( 58 mg , 0.24 mmol ) was added 1 - butyl - 3 - methylimidazolium hexa- fluorophosphate ( 2 mL ) as a solvent . The mixture was heated to 90 ° C under argon and monitored by TLC until the ...
... mmol ) and a soln of CAN ( 2.3–11.5 mmol ) in H2O ( 10–50 mL ) , and the mixture was stirred at rt . After completion of the reaction , the organic layer was separated , washed with brine , and dried ( Na2SO4 ) . The solvent was removed ...