Science of Synthesis: Houben-Weyl Methods of Molecular Transformations, 第 35 卷Ernst Schaumann Thieme, 2000 - 850 頁 Science of Synthesis: Houben-Weyl Methods of Molecular Transformations is the entirely new edition of the acclaimed reference series Houben-Weyl, the standard synthetic chemistry resource since 1909. This new edition is published in English and will comprise 48 volumes published between the years 2000 and 2008. Science of Synthesis is a quality reference work developed by a highly esteemed editorial board to provide a comprehensive and critical selection of reliable organic and organometallic synthetic methods. This unique resource is designed to be the first point of reference when searching for a synthesis strategy.
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... extracted with petro- leum ether . The organic extract was washed with H2O and sat . aq NaHCO3 and then dried ( Na2SO4 ) . The solvent was evaporated under reduced pressure to give the product ; yield of the isomeric products 43 ( R1 ...
... extracted with Et2O . The organic phases were dried ( Na2SO1 ) and the solvent was removed under reduced pressure ; yield : 350 mg ( 96 % ) . 35.2.5.2.10 Method 10 : Hydrobromination of Epoxides Using Lithium Tetrabromonickelate ( II ) ...
... extracted with CH2Cl2 ( 2 × ) , the combined organic layers were dried ( Na2SO ) , and the solvent was removed under reduced pressure . The crude product was purified by flash chromatogra- phy ; yield : 50–92 % . Iodohydrins 16 ...