Science of Synthesis: Houben-Weyl Methods of Molecular Transformations, 第 35 卷Ernst Schaumann Thieme, 2000 - 850 頁 Science of Synthesis: Houben-Weyl Methods of Molecular Transformations is the entirely new edition of the acclaimed reference series Houben-Weyl, the standard synthetic chemistry resource since 1909. This new edition is published in English and will comprise 48 volumes published between the years 2000 and 2008. Science of Synthesis is a quality reference work developed by a highly esteemed editorial board to provide a comprehensive and critical selection of reliable organic and organometallic synthetic methods. This unique resource is designed to be the first point of reference when searching for a synthesis strategy.
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... combined aqueous washings were back - extracted with CH2Cl2 ( 50 mL ) , and the total combined organic phase was washed with a sat . soln of NaCl and dried ( Na2SO4 ) . Distilla- tion ( 40-41 ° C / 6.5 Torr ) afforded the product ...
... combined organic layers were washed with brine ( 50 mL ) , and the brine layer was extracted with CH2Cl2 ( 2 × 20 mL ) . The combined organic layers were dried ( Na2SO4 ) and the solvent was removed under reduced pressure . The crude ...
... combined N2 / vacuum line , and a septum . Under N2 , a soln of MgBr , in Et2O was injected . Then , the alcohol was ... combination of bromotrimethylsilane and zinc ( II ) bromide permits the preparation of homoallylic bromides 25 from ...