Science of Synthesis: Houben-Weyl Methods of Molecular Transformations, 第 35 卷Ernst Schaumann Thieme, 2000 - 850 頁 Science of Synthesis: Houben-Weyl Methods of Molecular Transformations is the entirely new edition of the acclaimed reference series Houben-Weyl, the standard synthetic chemistry resource since 1909. This new edition is published in English and will comprise 48 volumes published between the years 2000 and 2008. Science of Synthesis is a quality reference work developed by a highly esteemed editorial board to provide a comprehensive and critical selection of reliable organic and organometallic synthetic methods. This unique resource is designed to be the first point of reference when searching for a synthesis strategy.
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第 1 到 3 筆結果,共 86 筆
... added dropwise to DMF ( 100 mL ) in a flask equipped with a N2 inlet , a magnetic stirrer , and a fractional distillation column . After the addition , stirring was discontinued and the thick , colorless solid that formed was allowed to ...
... added . After removal of the air , vinyl chloride ( 570 kg , 9194 mol ) was added and stirring was maintained at 56 ° C until the pressure was reduced to 0.5 MPa , indicating 85 % monomer consumption . After cooling , the product was ...
... added , under stirring and cooling ( < 10 ° C ) , a soln of Br2 ( 160 g , 1 mol ) in CCl4 ( 90 mL ) over 20 min . The solvent was removed by distillation and the crude product was distilled under reduced pressure ; yield : 210 g ( 85 ...