Science of Synthesis: Houben-Weyl Methods of Molecular Transformations, 第 35 卷Ernst Schaumann Thieme, 2000 - 850 頁 Science of Synthesis: Houben-Weyl Methods of Molecular Transformations is the entirely new edition of the acclaimed reference series Houben-Weyl, the standard synthetic chemistry resource since 1909. This new edition is published in English and will comprise 48 volumes published between the years 2000 and 2008. Science of Synthesis is a quality reference work developed by a highly esteemed editorial board to provide a comprehensive and critical selection of reliable organic and organometallic synthetic methods. This unique resource is designed to be the first point of reference when searching for a synthesis strategy.
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... Torr ) , the product was distilled ; yield : 32.7 g ( 90 % ) ; bp 65–70 ° C / 0.1 Torr . 35.1.1.5.2 Method 2 : Synthesis from Alkanesulfonates and a Source of Chloride lon Quite often alcohols are converted into chloroalkanes via the ...
... Torr ) ; the distillation was in- terrupted and the residue was recrystallized ( petroleum ether ) to give the product ; yield : not reported ; mp 64-65 ° C ; bp 183-185 ° C / 15 Torr . 4- ( Chloromethyl ) thiazole ( 12 ) : [ 12 ] ...
... Torr . 1,2 - Dibromoethyl Acetate ( 58 , R1 = H ) :( 167 ) CAUTION : Bromine is a severe irritant of the eyes , mucous membranes , lungs , and skin . Liquid bromine causes severe and painful burns on contact with eyes and skin . To a ...