Science of Synthesis: Houben-Weyl Methods of Molecular Transformations
Thieme, 2000 - 850 頁
New edition of the acclaimed reference series, Houben-Weyl. This new ed. is published in English and is available in both print and electronic formats. Clear and systematic, Science of Synthesis provides practical solutions and offers a route through the mass of information available in the primary literature. This one-stop reference tool is: Comprehensive: contains synthetic models selected by world-renowned experts, with full experimental procedures and background information. Reliable: the international editorial board is made up of distinguished chemists with unparalleled experience and competence. Logical and easy-to-navigate: information is organized in a hierarchical system based on the compound or functional group to be synthesized. Authoritative: critically evaluates the preparative applicability and significance of the synthetic methods. Wide-ranging: considers methods from journals, books, and patent literature from the early 1800s up to the present day and presents important synthetic methods for all classes of compounds.
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Abstr acetic achieved acid added addition affords alcohols aliphatic alkenes alkyl allylic amounts aqueous atom benzene benzyl bond bromine bromoalkanes carbon carbon tetrachloride catalyst CAUTION Chem chloride chloroalkanes chromatography combined complex compounds concentrated containing conversion cooled corresponding derivatives distilled dried Epoxides equiv esters ether example excess extracted filtrate flask formation formed functional give heated hydrogen bromide hydrogen chloride initiator intermediate iodide iodine iodoalkanes leads liquid MeCN metal Method methyl mixture mmol obtained organic layer oxide phosphorus prepared presence primary procedure proceeds purified radical Ratio react reaction reactivity reagent rearrangement reduced pressure reflux residue resulting ring opening salts Scheme secondary selective silica gel skin sodium soln solvent stirred substitution substrates Synth Synthesis Table temperature tertiary Tetrahedron Lett tion toxic treatment Typical undergo Variation washed yield